| dc.description.abstract | Crystallographic texture in polycrystalline materials are known to play an important role in tailoring suitable properties for various technological applications. In addition, the evolution of texture provides a profound basis to develop scientific understanding of physical processes occurring in the material during deformation and annealing. Between the two, the understanding of deformation texture is much broader. However, certain issues pertaining to the evolution of deformation texture evolution are yet to be explored or not uniquely agreed upon. A few notable examples are the effects of extreme grain sizes and strain rates. Moreover, most of the studies are pertaining to single phase metals and alloys. While many engineering alloys consist of two phase microstructures, the effect of second phase in the microstructure on the evolution of texture in the individual phases has not been studied in a comprehensive manner.
The present thesis is an attempt to addresses these issues in a more generic manner. The studies have been specifically aimed at examining the aforesaid issues in the close packed Face Centre Cubic (FCC) and Hexagonal Close Packed (HCP) metals and alloys. In brief, this thesis addresses the following problems pertaining to deformation texture: (i) the effect of extreme grain sizes, (ii) the effect of extreme strain rates and (iii) the effect of a second ductile phase.
Chapter 1 of the thesis gives a detailed survey of literature pertaining to the evolution of deformation textures in different metals and alloys, while chapter 2 includes the details of the experimental techniques and simulation procedures, which are mostly common for the entire work.
The issue of grain size is addressed in chapter 3. In the present investigation, the evolution of deformation texture in nickel (FCC) and titanium (HCP) with the extreme grain sizes (nanometre and millimetre) has been studied. Nanocrystalline nickel with the grain size ~ 20 nm was obtained by pulse electro-deposition while the other extreme of the grain size in nickel was obtained by annealing of a cold rolled sheet at 1373 K. The rolling texture in nanocrystalline nickel had a higher volume fraction of Brass component than in nickel with normal grain size. These results have been explained on the basis of inhibition of cross slip in small grain sizes and the operation of planar slip. This has been validated by viscoplastic self-consistent simulations. The texture of coarse grain nickel samples (typified as oligocrystalline, owing to the lesser number of grains in the thickness direction) also had higher Brass component like the nanocrystalline sample. A detailed analysis was performed by examining misorientation development in the grain interior and in the vicinity of the grain boundaries. The similarity at the two extreme length scales has been explained on the basis of lower “Grain Boundary Affected Zone” at the extreme length scales. To examine the effect of grain size in the case of HCP materials, commercially pure titanium with ultra-fine (500 nm) and normal grain size (~50 μm), was investigated. A monotonic evolution of texture was observed in the former, which has been attributed to the absence of twinning, a situation that could arise due to the lack of coordinated movement of twinning partials in the sub-micron grain size regime. Thus, a reasonable understanding of the evolution of deformation texture in hitherto unexplored regime of grain sizes was developed for the two materials.
The chapter 4 of the thesis is dedicated to the study of strain rate effects in both FCC and HCP materials. The issue of strain rate has been addressed by two ways: (a) deforming the materials at extreme strain rates, namely 10-3 s-1 to 10+3 s-1 under compression up to a reasonable strain, and (b) deforming the materials under torsion within a reasonable range of strain rates, but up to large strains. In this case, in addition to nickel, copper was also investigated owing to the different strain hardening behaviour of the two materials. The compression texture in nickel and copper was characterized by the presence of <101> component at low strain rates. At high strain rate, ~10+3 s-1, there was a decrease in the intensity of the <101> component for nickel but it strengthened for copper. This has been explained on the basis of continuous dynamic recrystallization in copper. The torsion texture evolution in nickel and copper was similar at low strain rate (10-3 s-1) and was characterized by the presence of important shear texture components. At high strain rate (1 s-1), texture weakened for nickel, while for copper a rotated cube component was observed which has been attributed to dynamic recrystallization.
The effect of strain rate was studied more comprehensively in hexagonal titanium by adding one more variable, that is, the initial texture. Extreme strain rates were imparted using static and dynamic compression tests. It was found that different initial textures led to different mechanical response in terms of yield strength and strain hardening as well as microstructural response in terms of twin fractions. The samples deformed at high strain rate showed increased twinning that led to some scatter in the texture components compared to low strain rate deformed samples. VPSC simulations were able to successfully capture the evolution of texture as well as microstructural evolution in terms of twin activity in the deformed samples at the extreme strain rates. Torsion tests on titanium at different strain rates indicated evolution of inhomogeneous nature of fibre texture components with increase in strain rate.
Thus, weakening of texture was observed irrespective of the strain path (compression or torsion) and crystal structure (FCC or HCP) unless additional restoration mechanism like recrystallization (continuous or discontinuous) intervened.
In chapter 5, the evolution of rolling texture in two phase FCC + BCC (Ni-Fe-Cr alloys) and HCP + BCC (Ti-13Nb-13Zr ) alloys has been studied. This study was aimed at examining the effect of second deforming phase on the texture evolution in the primary phase. The effect of various parameters like volume fraction and morphology of the second phase on deformation texture evolution was studied experimentally as well as by VPSC simulations. A reduction in the Brass component of texture was observed in the austenite phase due to the presence of harder ferrite phase while a characteristic rolling texture evolved in the ferrite phase. It has been established that the softer austenite phase carried maximum strain at low volume fractions of ferrite while the harder ferrite phase carried the maximum strain at higher volume fractions of ferrite.
In case of the two phase HCP+BCC alloy Ti-13Nb-13Zr, both the hexagonal α and the cubic β phases showed a characteristic rolling texture irrespective of two different morphologies. For both the equiaxed and colony microstructures, the softer β phase carried the maximum strain. VPSC simulations were able to model the deformation texture evolution as well as microstructural parameters like strain partitioning and twin fraction satisfactorily for both the microstructural conditions. It was found that the deformation mechanism in one phase could be affected by the presence of the second phase and that a characteristic change in deformation texture could be produced in the presence of the second phase. Thus, a comprehensive perspective has been developed pertaining to the evolution of texture in FCC and HCP phases in the presence of a second ductile phase.
The overall findings of the three investigations carried out for the thesis are summarised in chapter 6. | en_US |
